ASTM D3359, titled “Standard Test Methods for Measuring Adhesion by Tape Test,” provides a standardized procedure to evaluate the adhesion quality of a coating to its substrate. It’s widely employed in industries where paints and films are applied, ensuring they adhere properly to different surfaces. This testing method is particularly useful for quality control during the coating process, helping to identify potential adhesion failures early.
Coating adhesion affects the durability, performance, and lifespan of a product. Poor adhesion can lead to flaking, peeling, and cracking, which compromises both the aesthetic appeal and protective function of the coating. By conducting adhesion tests, manufacturers can:
ASTM D3359 specifies two main test methods for assessing paint and film adhesion:
In this method, a single X-shaped cut is made into the coating down to the substrate using a sharp blade. Pressure-sensitive tape is then applied over the cut and quickly removed. The adhesion is evaluated based on how much of the coating remains attached to the substrate after the tape is removed.
This method is suitable for coatings with a thickness of up to 125 micrometers (5 mils). It involves making a series of parallel cuts in the coating, followed by a second set of cuts intersecting the first set to form a grid pattern. Tape is then applied over the grid and removed to evaluate how much of the coating has detached. The adhesion is rated on a 0 to 5 scale, with 5 indicating perfect adhesion (no coating removed) and 0 indicating poor adhesion (more than 65% of the grid detached).
Here’s a quick overview of how to conduct an adhesion test according to ASTM D3359:
Prepare the Surface: Clean the coated surface to remove any contaminants, as they can affect adhesion.
Make the Cut: For Method A, use a sharp blade to create an X-cut in the coating. For Method B, use a specialized multi-blade tool to make a grid pattern.
Apply the Tape: Firmly press the pressure-sensitive tape over the cut or grid area. Ensure there are no air bubbles.
Remove the Tape: Quickly peel the tape back at a consistent angle (usually around 180°). The speed of removal is crucial to getting accurate results.
Assess the Results: Examine the amount of coating that has been removed from the substrate. For Method B, compare the remaining coating to the ASTM D3359 rating scale to determine adhesion quality.
Method A (X-Cut Test): The surface is examined visually, and the extent of coating removal is noted. Results are typically described qualitatively (e.g., “excellent,” “good,” “poor”).
Method B (Cross-Cut Test): The grid is examined, and the amount of coating removed is rated on a scale of 0 to 5:
ASTM D3359 is ideal for coatings applied to relatively flat surfaces where the thickness does not exceed 5 mils. It is commonly used in the following industries:
While ASTM D3359 is an effective and quick way to evaluate adhesion, it has limitations: